Synthesis of 14C‐labeled indole‐3‐acetylaspartic acid

Jerry D. Cohen

doi:10.1002/jlcr.2580180916

Synthesis of ¹⁴C‐labeled indole‐3‐acetylaspartic acid

Jerry D. Cohen

Horticultural Science

Research output: Contribution to journal › Comment/debate › peer-review

32 Scopus citations

Abstract

The synthesis of indole‐3‐acetyl‐2‐¹⁴C‐N‐aspartic acid from carrier‐free indole‐3‐acetic acid‐2‐¹⁴C (54.5 mCi/mmole) and bis‐t‐butyl‐l‐aspartic acid was accomplished by coupling with dicyclohexylcarbodiimide followed by removal of the ester blocking groups by treatment with 2 N NaOH.

Original language	English (US)
Pages (from-to)	1393-1396
Number of pages	4
Journal	Journal of Labelled Compounds and Radiopharmaceuticals
Volume	18
Issue number	9
DOIs	https://doi.org/10.1002/jlcr.2580180916
State	Published - Sep 1981

Keywords

Dicyclohexylcarbodiimide
indole‐3‐acetic acid
indole‐3‐acetylaspartic acid

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10.1002/jlcr.2580180916

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title = "Synthesis of 14C‐labeled indole‐3‐acetylaspartic acid",

abstract = "The synthesis of indole‐3‐acetyl‐2‐14C‐N‐aspartic acid from carrier‐free indole‐3‐acetic acid‐2‐14C (54.5 mCi/mmole) and bis‐t‐butyl‐l‐aspartic acid was accomplished by coupling with dicyclohexylcarbodiimide followed by removal of the ester blocking groups by treatment with 2 N NaOH.",

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AB - The synthesis of indole‐3‐acetyl‐2‐14C‐N‐aspartic acid from carrier‐free indole‐3‐acetic acid‐2‐14C (54.5 mCi/mmole) and bis‐t‐butyl‐l‐aspartic acid was accomplished by coupling with dicyclohexylcarbodiimide followed by removal of the ester blocking groups by treatment with 2 N NaOH.

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KW - indole‐3‐acetic acid

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